A Simple Key For tga66 Unveiled
A Simple Key For tga66 Unveiled
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The devices ended up connected to the respective spectrometers using a heated transfer line to prevent condensation on the off gases during the transfer. One exam was done around the FTIR at ambient atmosphere to collect the ATR-FTIR spectrum of your sample. TGA tests ended up carried out by heating the samples from ambient temperature to 1000 ˚C at ten ˚C/min on both of these techniques. About 2-3 mg of nylon sixty six was Utilized in each exam.
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The TGA-FTIR spectra of nylon 66 had been stored like a purpose of time within an array in a Gram Schmidt file. Because time and temperature could be very easily correlated within a TGA experiment, the TGA curve was analyzed to find out at what time the volatilization as well as the degradation took place. The Gram Schmidt file is plotted in eco-friendly in Figure 6 overlaying tga66 the TGA excess weight adjust as well as derivative curves.
TGA-FTIR spectra have been recorded during the TGA take a look at like a functionality of time and saved within an array because the Gram Schmidt file at Each individual knowledge point
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The TGA-FTIR outcomes compliment the TGA-MS benefits. Each techniques present beneficial details about the structures with the off-gasoline products with the nylon 66 thermal degradation process. FTIR can be quite helpful to establish the presence of sure chemical bonds and many practical teams in polymers. It really is widely employed for polymer characterization.